Aliphatic chains in calixarene derivatives

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Synthesis and reactions of large-ring spirodienone calixarene derivatives

The isomerism of the polyspirodienone derivatives of the large-ring p-fertbutylcalix[n]arenes (n=5,6,8) is analyzed. Monoand polyspirodienone calix[n]arene derivatives were prepared by mild oxidation of the respective calix[n]arenes and the obtained products were characterized. Reactions of the monospirodienone derivatives with hydrazines and their rearrangements to xanthenocalixarenes are desc...

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Transamidation, or the conversion of one amide to another, is a long-standing challenge in organic synthesis. Although notable progress has been made in the transamidation of primary amides, the transamidation of secondary amides has remained underdeveloped, especially when considering aliphatic substrates. Herein, we report a two-step approach to achieve the transamidation of secondary aliphat...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section A Foundations of Crystallography

سال: 1996

ISSN: 0108-7673

DOI: 10.1107/s0108767396088514